Due to the lack of structural data, the functional aspects of NLRP-signaling mechanism, which includes pathogen recognition, nucleotide-binding, and sensor-adaptor-effector interactions, are not fully understood.
deprotection. However, benzylidenes are usually hydrogenolyzed more slowly than benzyl ethers or olefins. OH RR 1 HO OO RR 1 OH RR 1 HO OO RR 1 n p-Methoxy Benzylidene Formation:See benzylidenes OH RR 1 HO OO RR 1 OMe BENZYLIDENE CONTINUED ON NEXT PAGE
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Deprotection of the twelve methoxyl groups was easily achieved by treatment with BBr3 and yielded the free-OH deltaarene derivative. Synthesis, Structures, and Properties of Core-Expanded Azacoronene Analogue: A Twisted π-System with Two N-Doped Heptagons
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-Deprotection is usually done under reductive conditions (H2-Pd/C, Na/NH3(l), electrolytic reduction, etc). Alternatively, benzyl groups can be deprotected by RuCl3/NaIO4 oxidation-then-hydrolysis or by the combination of a Lewis acid and a nucleophile (such as Me2BBr). General References.
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On: MeI, Me2SO4, Me3O BF4 Off: BBr3, TMSI, Benzyl ether (Bn). Off: H2, Pd/C - competitive (usually slower) than olefin reduction Lewis Acid: SN1 mechanism. deprotection K2CO3/MeOH H+ (TFA, HCl, TsOH). ortho esters: not electophilic, no acidic protons.